Effect of thermal annealing on the magnetic properties of Hastelloy C-276 alloy with intermediate Al2O3/Y2O3/MgO/LaMnO3 buffer layers
https://doi.org/10.26907/2541-7746.2025.2.397-408
Abstract
This article presents the results of an experimental study on the surface morphology, elemental composition, and magnetic properties of Hastelloy C-276 substrates with intermediate Al2O3/Y2O3/MgO/LaMnO3 buffer layers and a deposited MgB2 superconductor. Measurements were carried out at a magnetic field from −5 to 5 T and in the temperature interval from 5 to 15 K, with the annealing temperatures of the tapes in the range from 623 to 923 K. Vacuum annealing had a significant effect on the magnetic characteristics of the substrates, and the specific magnetic moment varied up to 20 % depending on the annealing temperature in the temperature interval from 5 to 15 K.
Keywords
About the Authors
I. V. YanilkinRussian Federation
Igor V. Yanilkin, Cand. Sci. (Engineering), Senior Researcher, Institute of Physics
Kazan
A. I. Gumarov
Russian Federation
Amir I. Gumarov, Senior Researcher, Institute of Physics
Kazan
D. S. Uvin
Russian Federation
Denis S. Uvin, Junior Researcher, Institute of Physics
Kazan
A. G. Kiiamov
Russian Federation
Airat G. Kiiamov, Cand. Sci. (Physics and Mathematics), Leading Researcher, Institute of Physics
Kazan
S. A. Khokhorin
Russian Federation
Savely A. Khokhorin, Student
St. Petersburg
R. G. Batulin
Russian Federation
Ruslan G. Batulin, Cand. Sci. (Physics and Mathematics), Associate Professor, Institute of Physics
Kazan
References
1. Batulin R., Cherosov M., Kiiamov A., Rudnev I., Khokhorin S., Uvin D., Rogov A., Tayurskii D. The physical properties of Hastelloy® C-276TM and Hastelloy® C-276TM with Al2O3/Y2O3/MgO/LaMnO3 buffer layers down to cryogenic temperatures for applications in superconducting magnets // Cryogenics. 2023. V. 137. Art. 103776. https://doi.org/10.1016/j.cryogenics.2023.103776.
2. Lu J., Choi E.S., Zhou H.D. Physical properties of Hastelloy® C-276TM at cryogenic tempera- tures // J. Appl. Phys. 2008. V. 103, No 6. Art. 064908. https://doi.org/10.1063/1.2899058.
3. Lee S., Petrykin V., Molodyk A., Samoilenkov S., Kaul A., Vavilov A., Vysotsky V., Fetisov S. Development and production of second generation high Тс superconducting tapes at SuperOx and first tests of model cables // Supercond. Sci. Technol. 2014. V. 27, No 4. Art. 044022. https://doi.org/10.1088/0953-2048/27/4/044022.
4. Zhao Y., Zhu J.-M., Jiang G.-Y., Chen C.-S., Wu W., Zhang Z.-W., Chen S.-K., Hong Y.M., Hong Z.-Y., Jin Z.-J. Progress in fabrication of second generation high temperature supercon- ducting tape at Shanghai Superconductor Technology // Supercond. Sci. Technol. 2019. V. 32, No 4. Art. 044004. https://doi.org/10.1088/1361-6668/aafea5.
5. Wang K., Dong H., Huang D., Shang H., Xie B., Zou Q., Zhang L., Feng C., Gu H., Ding F. Advances in second-generation high-temperature superconducting tapes and their applications in high-field magnets // Soft Sci. 2022. V. 2, No 3. Art. 12. https://doi.org/10.20517/ss.2022.10.
6. Rudnev I., Abin D., Pokrovskii S., Anishchenko I., Starikovskii A., Osipov M. Influence of ion irradiation on critical characteristics of second-generation HTSC tapes // IEEE Trans. Appl. Supercond. 2022. V. 32, No 4. Art. 8000905. https://doi.org/10.1109/TASC.2022.3164629.
7. Chen Z., Calvi M., Durrell J., Boffo C., Wei D., Zhang K., Zhao Z. Recent progress in high-temperature superconducting undulators // Superconductivity. 2024. V. 12. Art. 100134. https://doi.org/10.1016/j.supcon.2024.100134.
8. Hata S., Sosiati H., Kuwano N., Tomokiyo Y., Matsumoto A., Fukutomi M., Kitaguchi H., Komori K., Kumakura H. Effects of heat treatments on microstructure formation in MgB2 /YSZ/Hastelloy film // IEEE Trans. Appl. Supercond. 2005. V. 15, No 2. P. 3238–3241. https://doi.org/10.1109/TASC.2005.848834.
9. Putri W.B.K., Kang B., Van Duong P., Kang W.N. Reducing delamination in MgB2 films deposited on Hastelloy tapes by applying SiC buffer layers // Thin Solid Films. 2015. V. 590. P. 80–83. https://doi.org/10.1016/j.tsf.2015.07.057.
10. Kang B., Putri W.B.K., Kang W.N. Effect of SiC buffer layer on flux pinning property of MgB2 tapes // Curr. Appl. Phys. 2019. V. 19, No 6. P. 670–674. https://doi.org/10.1016/j.cap.2019.03.012.
11. Zhang X.Y., Zhong J., Guo S., Zhao J. Control of deformation and annealing process to produce incoherent Σ3 boundaries in Hastelloy C-276 alloy // Nucl. Mater. Energy. 2021. V. 27. Art. 100944. https://doi.org/10.1016/j.nme.2021.100944.
12. Kumar G.S., Sivamaran V., Lokanadham R., Raju C., Mandal T.K. Influence of heat treatment on microstructure and mechanical properties of pulsed Nd:YAG laser welded dissimilar sheets of Hastelloy C-276 and monel 400 // Phys. Scr. 2023. V. 98, No 9. Art. 095933. https://doi.org/10.1088/1402-4896/aceb3b.
13. Zhang C., Zhang L., Cui Y., Feng Q., Cheng C. Effects of high-temperature aging on precipitation and corrosion behavior of a Ni-Cr-Mo-based Hastelloy C276 superalloy // J. Mater. Eng. Perform. 2020. V. 29, No 3. P. 2026–2034. https://doi.org/10.1007/s11665-020-04723-y.
14. Yanilkin I.V., Gumarov A.I., Rudnev I.A., Fatikhova L.R., Kiiamov A.G., Denisov A.E., Khokhorin S.A., Tayurskii D.A., Batulin R.G. Synthesis of MgB2 films on Hastelloy-C276 tape with Al2O3/Y2O3/MgO/LaMnO3 buffer layers by magnetron sputtering in co-evaporation mode // Supercond. Sci. Technol. 2024. V. 37, No 8. Art. 085015. https://doi.org/10.1088/1361-6668/ad5c09.
15. Balcells L., Beltr´an J.I., Mart´ınez-Boubeta C., Konstantinovi´c Z., Arbiol J., Mart´ınez B. Aging of magnetic properties in MgO films // Appl. Phys. Lett. 2010. V. 97, No 25. Art. 252503. https://doi.org/10.1063/1.3527963.
16. Yufeng C., Wang G., Zhengfeng S., Shenggao W., Yangwu M., Quanrong D., Jingjing Y. Magnetic characteristics of LaMnO3+𝛼 thin films deposited by RF magnetron sputtering in an O 2 /Ar mixture gas // Mater. Res. Express. 2021. V. 8, No 1. Art. 016101. https://doi.org/10.1088/2053-1591/abd6a3.
17. Kim H.S., Christen H.M. Controlling the magnetic properties of LaMnO3 thin films on SrTiO3(100) by deposition in a O 2 /Ar gas mixture // J. Phys.: Condens. Matter. 2010. V. 22, No 14. Art. 146007. https://doi.org/10.1088/0953-8984/22/14/146007.
18. Atamert S., Bhadeshia H.K.D.H. Nickel based hardfacing alloys for high temperature applications // Mater. Sci. Technol. 1989. V. 5, No 12. P. 1220–1228. https://doi.org/10.1179/mst.1989.5.12.1220.
Review
For citations:
Yanilkin I.V., Gumarov A.I., Uvin D.S., Kiiamov A.G., Khokhorin S.A., Batulin R.G. Effect of thermal annealing on the magnetic properties of Hastelloy C-276 alloy with intermediate Al2O3/Y2O3/MgO/LaMnO3 buffer layers. Uchenye Zapiski Kazanskogo Universiteta. Seriya Fiziko-Matematicheskie Nauki. 2025;167(2):397-408. (In Russ.) https://doi.org/10.26907/2541-7746.2025.2.397-408